[SI-LIST] Re: Effects of steam?

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Hi all,

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Two electrochemical reactions can happen in pcb=2E

1=2E    Dendrite formation

2=2E    Conductive filament formation=2E

=20

Dendrites are formed on the surface and they propagate from cathode to=
 anode whereas CFF is formed between vias to vias, layers to layers, track=
 to via and track to track and they propagate from anode to cathode=2E

=20

Please find the attached file, which explains conductive filament formation=
 (CFF) or conductive anodic filament (CAF) formation=2E We have similar=
 kind problem like CFF in our boards=2E Currently we are debugging it=2E=
 Our boards are burning at the input power connector due to heat=
 dissipation (even bare boards without any components)=2E=20

=20

Lot of literature is available in the internet, simply Google it on=
 conductive filament formation in pcb=2E

=20

http://www=2Eami=2Eac=2Euk/courses/topics/0152_caf/index=2Ehtml

=20

=20

Hope this information is useful=2E Please share your experience on CFF=2E

=20

Thanks

Uma

-----Original Message-----
From: si-list-bounce@freelists=2Eorg [mailto:si-list-bounce@freelists=
=2Eorg] On Behalf Of Richard Jungert
Sent: Tuesday, November 25, 2008 7:22 AM
To: howie03@sigcon=2Ecom; si list freelist
Subject: [SI-LIST] Re: Effects of steam?

=20

John=2E

=20

Do research on Dendrite formation in the presence of moisture on printed=
 circuit boards=2E=20

Here is some info I have found recently=2E=20

Residues left on the boards during the printed board manufacturing stages=
 can also lead to dendrite formation=2E=20

A copper dendrite is the most common found on a

printed circuit board assembly, dendrites however can be silver, tin,=
 copper or

other metallic materials=2E They occur when contamination is present on the

surface of printed board in the presence of moisture, equally it can be=
 found

on other surfaces like on a ceramic substrate in a hybrid circuit or even=
 on

the surface of a component between two terminations=2E Lowering of surface

resistance between a track and pad or track and via hole and can lead to

corrosion=2E This often results in the formation of metal filaments just=
 like a

fern or Christmas tree=2E Electrochemical reaction dissolves metal at one

electrode and forms at the opposite electrode=2E Often but not always they=
 form

from the anode to cathode=2E

=20

Moisture can cause lots of problems like this too=2E

=20

Richard Jungert

=20

> From: howie03@sigcon=2Ecom

> To: si-list@freelists=2Eorg

> Subject: [SI-LIST] Re: Effects of steam?

> Date: Mon, 24 Nov 2008 13:29:46 -0800

>=20

> Dear John Barrett,

>=20

> I don't have exact numbers, but I think the problem will be much worse=
 that

> you imagine=2E   Here is my reasoning=2E=20

>=20

> (1) Water can (apparently) induce some types of lamination failure=2E To

> address that problem, board manufacturers long ago agreed to a standard

> delamination test for water absorbtion=2E  In this test, if I remember it

> correctly, the finished pcb is subjected to a hot, high humidity

> environment=2E  Then you try to pull the board apart (de-laminating it)=
 with

> suction cups=2E  Anyway, after processing, the board can also be weighed=
 to

> determine the percentage water absorption=2E  That's what you want to=
 know=2E I

> remember figures like 1% being rated as "OK" for pcb laminates (please=
 check

> the number with your board supplier)=2E

>=20

> (2) I do not know the density of your board material, but if I did, I=
 would

> take the percentage water absorption by weight and from it compute the

> percentage water BY VOLUME, which is what counts=2E  Call that percentage

> "alpha"=2E

>=20

> (3) The complex dielectric permittivity of your wet board may be

> approximated by the following equation=2E This equation takes into=
 account

> both the real and imaginary parts of permittivity=2E =20

>     E(wet) =3D (1-alpha)E[polyimide] + (alpha)E[water]

>=20

> (4) Now we get to the interesting part=2E The complex dielectric=
 permittivity

> of water has a magnitude of about 80 (eighty), and a terrible loss=
 tangent

> (don't recall how bad -- but this is part of the reason microwave ovens=
 work

> so well)=2E  Since the magnitude of E[water] is so huge (80), it doesn't=
 take

> much of an "alpha" to significantly degrade the properties of your=
 laminate=2E

>=20

>=20

> For example, (please don't quote these numbers this is just an example):

> Park Nelco N7000 polyimide resin/e-glass:  E[polyimide] =3D 3=2E8*(1 - 0=
=2E016j)

> Water:  E[water] =3D 80*(1 - 0=2E2j)  (just a guess for this example)

> Alpha=3D0=2E01 (one-percent absorbtion)

> Result: E[wet] =3D 0=2E99*3=2E8*(1 - 0=2E016j) + 0=2E01*80*(1 - 0=2E2j) =
=20

>                =3D 3=2E762 - 0=2E0608j       + 0=2E80 - 0=2E16j

>                =3D 4=2E562 - =2E2208 =20

> The loss tan of the result is =2E2208/4=2E562 =3D 0=2E048, triple the=
 original

> figure=2E

>=20

> The water component, even if it doesn't change the overall dielectric

> constant very much, can change the loss tangent a lot=2E=20

>=20

> RELATED ISSUE: People who make low-loss capacitors keep their materials=
 dry=2E

> That seems closely related to your issue=2E The following designers guide=
 for

> capacitors says, "Water in printed circuit laminates is responsible for a

> form of dielectric absorption called "hook" that causes many problems for

> users of high impedance and high frequency attenuators=2E"

>         http://www=2Edesigners-guide=2Eorg/Modeling/da=2Epdf=20

>=20

>=20

> I hope these brief comments are helpful to you=2E

>=20

> If anyone has the dielectric loss numbers for water, I'd like to see=
 them,

> please=2E=20

>=20

> Best regards,

> Dr=2E Howard Johnson, Signal Consulting Inc=2E,

> tel +1 509-997-0505,  howie03@sigcon=2Ecom

> www=2Esigcon=2Ecom -- High-Speed Digital Design seminars, publications=
 and films

> =20

>=20

>=20

>=20

>=20

> -----Original Message-----

> From: si-list-bounce@freelists=2Eorg [mailto:si-list-bounce@freelists=
=2Eorg] On

> Behalf Of John Barrett

> Sent: Monday, November 24, 2008 4:09 AM

> To: si-list@freelists=2Eorg

> Subject: [SI-LIST] Effects of steam?

>=20

> This one is a bit off the beaten track but I want to operate an organic

> circuit board (no devices, just gold conductors on polyimide), in an

> autoclave with high pressure (3 bar), high temperature (135C)=
 non-saturated

> steam=2E There's no condensation and so no real water about=2E What would=
 be the

> effect of steam absorption on the dielectric constant and the loss=
 tangent

> up to 5GHz?=20

> =20

>=20

> Non-saturated steam, i=2Ee=2E dry, invisible steam, has dielectric=
 properties

> very close to air so, if it were to penetrate a porous material e=2Eg=2E=
 porous

> alumina, then it would just displace the air in the pores and cause=
 little

> variation in electrical parameters=2E With something like polyimide,=
 which I

> presume absorbs moisture inter-molecularly, there are measureable shifts=
 in

> dielectric properties with variations in moisture content caused by=
 humidity

> variations at normal temperatures, and I think that this is caused by the

> release of extra charges, but what are the effects in 135C, 3bar steam? I

> could measure the effects with resonator test structures and a VNA but I

> would need to find and invest in high frequency connectors and cables=
 able

> to withstand the autoclave atmosphere - not cheap, I imagine, even if=
 they

> exist=2E Perhaps there are dielectric experts on the list who might be=
 able to

> speculate from a materials science viewpoint?

>=20

> =20

>=20

> Regards and thanks,

>=20

> =20

>=20

> John

>=20

> =20

>=20

> S=E9an de Bar=F3id                    =20

>=20

> Ionad um Raidich=F3rais Inoiri=FAnaithe

> Roinn na hInnealt=F3ireachta Leictreona=ED

> Institi=FAd Teicneola=EDochta Chorca=ED   =20

>=20

>                          =20

> ________________

> John Barrett

>=20

> Centre for Adaptive Wireless Systems

> Department of Electronic Engineering

> Cork Institute of Technology

>=20

> "Beidh f=E1ilte roimh freagra as Gaeilge"

>=20

> =20

>=20

>=20

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